N-Doped Mesoporous Carbon As a New Sorbent for Ultrasonic-Assisted Dispersive Micro-Solid-Phase Extraction of 1-Naphthol and 2-Naphthol, the Biomarkers of Exposure to Naphthalene, From Urine Samples

N-Doped Mesoporous Carbon As a New Sorbent for Ultrasonic-Assisted Dispersive Micro-Solid-Phase Extraction of 1-Naphthol and 2-Naphthol, the Biomarkers of Exposure to Naphthalene, From Urine Samples Publisher Pubmed

Omidi F¹ ; Dehghani F² ; Jamaleddin Shahtaheri S^{3, 4}

Show Affiliations

1. Research Center for Environmental Determinants of Health (RCEDH), Health Institute, Kermanshah University of Medical Sciences, Kermanshah, Iran
2. Department of Occupational Health Engineering, School of Public Health, Shiraz University of Medical Sciences, Shiraz, Iran
3. Department of Occupational Health Engineering, School of Public Health, Tehran University of Medical Sciences, Tehran, Iran
4. Institute for Environmental Research, Tehran University of Medical Sciences, Tehran, Iran

Source: Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences Published:2020

Abstract

This study aimed to optimize a new sample preparation method using N-doped mesoporous carbon sorbent for simultaneous measurement of 1-naphthol and 2-naphthol, the biomarkers of exposure to naphthalene. The samples were analyzed using high-performance liquid chromatography supplied with ultraviolet detector (HPLC-UV). N-doped mesoporous carbon sorbent was obtained via the hard template procedure. The synthesized nanosorbent was then characterized by transmission electron microscopy (TEM), Brunauer-Emmett-Teller (BET), and elemental analysis (CHN). The effective factors in the extraction of the studied biomarkers were examined by the Box-Behnken (BBD) methodology. Regarding the optimum conditions, the sketched calibration curve for naphthols was linear in the concentration levels of 1–600 µg L-1 for human urine samples. The accuracy and reproducibility of the introduced method were determined using the relative recovery (RR %) and relative standard deviation (RSD %) tests on the fortified urine samples. RR% and RSD% were found to be 97.0–101.2% and 3.1–9.0%, respectively. The calculated method detection limit of the optimized procedure was 0.3 µg L-1 and 0.5 µg L-1 for 1-naphthol and 2-naphthol, respectively. © 2020 Elsevier B.V.

2. Application of Ultrasonication for Facilitating the Extraction of Hippuric Acid and Methyl Hippuric Acid in Real Samples Using Fe3o4@Sio2@Sodium Dodecyl Sulfate: Experimental Design Methodology, Analytical Methods (2018)

3. Air-Assisted in Situ Deep Eutectic Solvent Decomposition Followed by the Solidification of Floating Organic Droplets-Liquid-Liquid Microextraction Method for Extraction of Azole Antifungal Drugs in Biological Samples Prior to High-Performance Liquid Chromatography, Journal of Separation Science (2022)

4. Application of Metal–Organic Frameworks in Novel Sample Pretreatment Techniques for Occupational Exposure Biomonitoring: A Review, Chemical Papers (2023)

5. Development of Dispersive Liquid-Liquid Microextraction Procedure for Trace Determination of Malathion Pesticide in Urine Samples, Iranian Journal of Public Health (2019)

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Seyed Jamaledin Shataheri (4)

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Style	Citing Format
MLA	Omidi F, Dehghani F, Jamaleddin Shahtaheri S. "N-Doped Mesoporous Carbon As a New Sorbent for Ultrasonic-Assisted Dispersive Micro-Solid-Phase Extraction of 1-Naphthol and 2-Naphthol, the Biomarkers of Exposure to Naphthalene, From Urine Samples." Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences, vol. 1160, no. , 2020, pp. -.
APA	Omidi F, Dehghani F, Jamaleddin Shahtaheri S (2020). N-Doped Mesoporous Carbon As a New Sorbent for Ultrasonic-Assisted Dispersive Micro-Solid-Phase Extraction of 1-Naphthol and 2-Naphthol, the Biomarkers of Exposure to Naphthalene, From Urine Samples. Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences, 1160(), -.
Chicago	Omidi F, Dehghani F, Jamaleddin Shahtaheri S. "N-Doped Mesoporous Carbon As a New Sorbent for Ultrasonic-Assisted Dispersive Micro-Solid-Phase Extraction of 1-Naphthol and 2-Naphthol, the Biomarkers of Exposure to Naphthalene, From Urine Samples." Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences 1160, no. (2020): -.
Harvard	Omidi F, Dehghani F, Jamaleddin Shahtaheri S (2020) 'N-Doped Mesoporous Carbon As a New Sorbent for Ultrasonic-Assisted Dispersive Micro-Solid-Phase Extraction of 1-Naphthol and 2-Naphthol, the Biomarkers of Exposure to Naphthalene, From Urine Samples', Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences, 1160(), pp. -.
Vancouver	Omidi F, Dehghani F, Jamaleddin Shahtaheri S. N-Doped Mesoporous Carbon As a New Sorbent for Ultrasonic-Assisted Dispersive Micro-Solid-Phase Extraction of 1-Naphthol and 2-Naphthol, the Biomarkers of Exposure to Naphthalene, From Urine Samples. Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences. 2020;1160():-.
BibTex	@article{ author = {Omidi F and Dehghani F and Jamaleddin Shahtaheri S}, title = {N-Doped Mesoporous Carbon As a New Sorbent for Ultrasonic-Assisted Dispersive Micro-Solid-Phase Extraction of 1-Naphthol and 2-Naphthol, the Biomarkers of Exposure to Naphthalene, From Urine Samples}, journal = {Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences}, volume = {1160}, number = {}, pages = {-}, year = {2020} }
RIS	TY - JOUR AU - Omidi F AU - Dehghani F AU - Jamaleddin Shahtaheri S TI - N-Doped Mesoporous Carbon As a New Sorbent for Ultrasonic-Assisted Dispersive Micro-Solid-Phase Extraction of 1-Naphthol and 2-Naphthol, the Biomarkers of Exposure to Naphthalene, From Urine Samples JO - Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences VL - 1160 IS - SP - EP - PY - 2020 ER -

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