Synthesis of Carbon Energized Materials With Directed Regulation of Specific Surface and Pore Structure As Potential Adsorbent for Methane Mitigation

Synthesis of Carbon Energized Materials With Directed Regulation of Specific Surface and Pore Structure As Potential Adsorbent for Methane Mitigation Publisher

Memetova A¹ ; Tyagi I² ; Karri RR³ ; Singh P⁵ ; Goscianska J⁶ ; Memetov N¹ ; Zelenin A¹ ; Gerasimova A¹ ; Tkachev A¹ ; Babkin A⁷ ; Shuklinov A⁸ ; Dehghani MH^{9, 10} ; Agarwal S¹¹

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1. Department of Technology and Methods of Nanoproducts Manufacturing, Tambov State Technical University, 106 Sovetskaya St, Tambov, 392000, Russian Federation
2. Centre for Dna Taxonomy, Molecular Systematics Division, Zoological Survey of India, Kolkata, 700 053, India
3. Petroleum and Chemical Engineering, Faculty of Engineering, Universiti Teknologi Brunei, Bandar Seri Begawan, BE1410, Brunei Darussalam
4. Department of Chemistry, Gurukul Kangri (Deemed to Be University), Hardwar, 249404, India
5. Department of Chemistry, University of Delhi, New Delhi, 110007, India
6. Department of Chemical Technology, Faculty of Chemistry, Adam Mickiewicz University in Poznan, Uniwersytetu Poznanskiego 8, Poznan, 61-614, Poland
7. Department of Chemistry, Lomonosov Moscow State University, Leninskie Gory 1-3, Moscow, 119991, Russian Federation
8. Testing Center, Tambov State University Named by G.R. Derzhavin, 33 Internatsional'naya St, Tambov, 392000, Russian Federation
9. Department of Environmental Health Engineering, School of Public Health, Tehran University of Medical Sciences, Tehran, Iran
10. Institute for Environmental Research, Center for Solid Waste Research, Tehran University of Medical Sciences, Tehran, Iran
11. Center for Excellence for Advanced Materials Research, King Abdulaziz University, Jeddah, 21589, Saudi Arabia

Source: Journal of Environmental Chemical Engineering Published:2022

Abstract

In this study, nanoporous carbon material (NCM) specimens were synthesized from polymer raw materials (a mixture of furfural, hydroquinone, and urotropine). The influence of the conditions and parameters of the synthesis method (temperature, weight ratio of the activating agent to the precursor and contact time) on the NCM structure was examined. The effect of the weight ratio of the initial components on the properties of the resulting NCM was investigated, and the optimal composition of the ternary system of furfural, hydroquinone and urotropine was found. The results of nitrogen adsorption-desorption showed that NCM specimens obtained by varying the activation temperature were microporous but with different micropore volumes and the same pore size distribution. Varying the weight ratio of the activating agent (KOH) to the precursor made it possible to obtain microporous, micromesoporous, and mesoporous NCMs. NCM specimens with different pore hierarchy and different specific surface area were also obtained, including microporous NCMs (SBET: 1546-3030 m3/g; Vmic/Vt: 76.0-100%), micro- mesoporous NCMs (SBET: 3204-3516 m3/g; Vmic/Vt: 41.2-57.4% Vmes/Vt: 42.6-58.8%) and mesoporous NCMs (SBET: 3641-3649 m3/g; Vmes/Vt: 74.0-83.8%). Further, a mechanism for the development of pores during KOH activation of polymeric carbon precursor was proposed. The outcomes of this study signify that the NCM5/750/1 has a high adsorption capacity for CH4 and has good prospects for monitoring CH4 emissions and reducing greenhouse gas emissions. © 2022 Elsevier Ltd.

2. Methods for Preparation and Activation of Activated Carbon: A Review, Environmental Chemistry Letters (2020)

3. Preparation, Characterization and Cr(Vi) Adsorption Evaluation of Naoh-Activated Carbon Produced From Date Press Cake; an Agro-Industrial Waste, Bioresource Technology (2018)

Experts (# of related papers)

Mohammadhadi Dehghani Tafti (2)

Style	Citing Format
MLA	Memetova A, et al.. "Synthesis of Carbon Energized Materials With Directed Regulation of Specific Surface and Pore Structure As Potential Adsorbent for Methane Mitigation." Journal of Environmental Chemical Engineering, vol. 10, no. 6, 2022, pp. -.
APA	Memetova A, Tyagi I, Karri RR, Singh P, Goscianska J, Memetov N, Zelenin A, Gerasimova A, Tkachev A, Babkin A, Shuklinov A, Dehghani MH, Agarwal S (2022). Synthesis of Carbon Energized Materials With Directed Regulation of Specific Surface and Pore Structure As Potential Adsorbent for Methane Mitigation. Journal of Environmental Chemical Engineering, 10(6), -.
Chicago	Memetova A, Tyagi I, Karri RR, Singh P, Goscianska J, Memetov N, Zelenin A, et al.. "Synthesis of Carbon Energized Materials With Directed Regulation of Specific Surface and Pore Structure As Potential Adsorbent for Methane Mitigation." Journal of Environmental Chemical Engineering 10, no. 6 (2022): -.
Harvard	Memetova A et al. (2022) 'Synthesis of Carbon Energized Materials With Directed Regulation of Specific Surface and Pore Structure As Potential Adsorbent for Methane Mitigation', Journal of Environmental Chemical Engineering, 10(6), pp. -.
Vancouver	Memetova A, Tyagi I, Karri RR, Singh P, Goscianska J, Memetov N, et al.. Synthesis of Carbon Energized Materials With Directed Regulation of Specific Surface and Pore Structure As Potential Adsorbent for Methane Mitigation. Journal of Environmental Chemical Engineering. 2022;10(6):-.
BibTex	@article{ author = {Memetova A and Tyagi I and Karri RR and Singh P and Goscianska J and Memetov N and Zelenin A and Gerasimova A and Tkachev A and Babkin A and Shuklinov A and Dehghani MH and Agarwal S}, title = {Synthesis of Carbon Energized Materials With Directed Regulation of Specific Surface and Pore Structure As Potential Adsorbent for Methane Mitigation}, journal = {Journal of Environmental Chemical Engineering}, volume = {10}, number = {6}, pages = {-}, year = {2022} }
RIS	TY - JOUR AU - Memetova A AU - Tyagi I AU - Karri RR AU - Singh P AU - Goscianska J AU - Memetov N AU - Zelenin A AU - Gerasimova A AU - Tkachev A AU - Babkin A AU - Shuklinov A AU - Dehghani MH AU - Agarwal S TI - Synthesis of Carbon Energized Materials With Directed Regulation of Specific Surface and Pore Structure As Potential Adsorbent for Methane Mitigation JO - Journal of Environmental Chemical Engineering VL - 10 IS - 6 SP - EP - PY - 2022 ER -

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