Application of Polyaniline–Multiwalled Carbon Nanotubes Composite Fiber for Determination of Benzaldehyde in Injectable Pharmaceutical Formulations by Solid-Phase Microextraction Gc

Application of Polyaniline–Multiwalled Carbon Nanotubes Composite Fiber for Determination of Benzaldehyde in Injectable Pharmaceutical Formulations by Solid-Phase Microextraction Gc–Fid Using Experimental Design Publisher

Masoumi V¹ ; Mohammadi A^{1, 2} ; Khoshayand MR^{1, 3} ; Ansari M⁴

Show Affiliations

1. Department of Drug and Food Control, Faculty of Pharmacy, Tehran University of Medical Sciences, P.O. Box 14155â€“645, Tehran, Iran
2. Nanotechnology Research Centre, Faculty of Pharmacy, Tehran University of Medical Sciences, P.O. Box 14155â€“645, Tehran, Iran
3. Pharmaceutical quality assurance research Centre, Faculty of Pharmacy, Tehran University of Medical Sciences, P.O. Box 14155â€“645, Tehran, Iran
4. Faculty of Pharmacy, Kerman University of Medical Sciences, Kerman, Iran

Source: Journal of Analytical Chemistry Published:2017

Abstract

A polyaniline–multiwalled carbon nanotubes composite fiber was electrodeposited onto a platinum wire using cyclic voltammetry. This fiber was used for headspace solid-phase microextraction combined with gas chromatography and flame ionization detector of trace levels of benzaldehyde in some injectable pharmaceutical formulations. Three solid-phase microextraction parameters including temperature, time and stirring rate were investigated simultaneously using a three-level-three-factor Box–Behnken as experimental design on the extraction capability. The as-made fiber has a lifetime of over 300 extractions without any obvious decline in extraction efficiency. At the optimum conditions (extraction temperature 60°C, extraction time 15 min, stirring rate 700 rpm), the method displays excellent linearity over the concentration range of 25–1000 ng/mL of benzaldehyde with RSD values ranging from 1.0 to 6.8%. The limits of quantitation and detection were 25 and 10 ng/mL, respectively. © 2017, Pleiades Publishing, Ltd.

Style	Citing Format
MLA	Masoumi V, et al.. "Application of Polyaniline–Multiwalled Carbon Nanotubes Composite Fiber for Determination of Benzaldehyde in Injectable Pharmaceutical Formulations by Solid-Phase Microextraction Gc–Fid Using Experimental Design." Journal of Analytical Chemistry, vol. 72, no. 3, 2017, pp. 264-271.
APA	Masoumi V, Mohammadi A, Khoshayand MR, Ansari M (2017). Application of Polyaniline–Multiwalled Carbon Nanotubes Composite Fiber for Determination of Benzaldehyde in Injectable Pharmaceutical Formulations by Solid-Phase Microextraction Gc–Fid Using Experimental Design. Journal of Analytical Chemistry, 72(3), 264-271.
Chicago	Masoumi V, Mohammadi A, Khoshayand MR, Ansari M. "Application of Polyaniline–Multiwalled Carbon Nanotubes Composite Fiber for Determination of Benzaldehyde in Injectable Pharmaceutical Formulations by Solid-Phase Microextraction Gc–Fid Using Experimental Design." Journal of Analytical Chemistry 72, no. 3 (2017): 264-271.
Harvard	Masoumi V et al. (2017) 'Application of Polyaniline–Multiwalled Carbon Nanotubes Composite Fiber for Determination of Benzaldehyde in Injectable Pharmaceutical Formulations by Solid-Phase Microextraction Gc–Fid Using Experimental Design', Journal of Analytical Chemistry, 72(3), pp. 264-271.
Vancouver	Masoumi V, Mohammadi A, Khoshayand MR, Ansari M. Application of Polyaniline–Multiwalled Carbon Nanotubes Composite Fiber for Determination of Benzaldehyde in Injectable Pharmaceutical Formulations by Solid-Phase Microextraction Gc–Fid Using Experimental Design. Journal of Analytical Chemistry. 2017;72(3):264-271.
BibTex	@article{ author = {Masoumi V and Mohammadi A and Khoshayand MR and Ansari M}, title = {Application of Polyaniline–Multiwalled Carbon Nanotubes Composite Fiber for Determination of Benzaldehyde in Injectable Pharmaceutical Formulations by Solid-Phase Microextraction Gc–Fid Using Experimental Design}, journal = {Journal of Analytical Chemistry}, volume = {72}, number = {3}, pages = {264-271}, year = {2017} }
RIS	TY - JOUR AU - Masoumi V AU - Mohammadi A AU - Khoshayand MR AU - Ansari M TI - Application of Polyaniline–Multiwalled Carbon Nanotubes Composite Fiber for Determination of Benzaldehyde in Injectable Pharmaceutical Formulations by Solid-Phase Microextraction Gc–Fid Using Experimental Design JO - Journal of Analytical Chemistry VL - 72 IS - 3 SP - 264 EP - 271 PY - 2017 ER -

Style

Citing Format

MLA

Masoumi V, et al.. "Application of Polyaniline–Multiwalled Carbon Nanotubes Composite Fiber for Determination of Benzaldehyde in Injectable Pharmaceutical Formulations by Solid-Phase Microextraction Gc–Fid Using Experimental Design." Journal of Analytical Chemistry, vol. 72, no. 3, 2017, pp. 264-271.

APA

Masoumi V, Mohammadi A, Khoshayand MR, Ansari M (2017). Application of Polyaniline–Multiwalled Carbon Nanotubes Composite Fiber for Determination of Benzaldehyde in Injectable Pharmaceutical Formulations by Solid-Phase Microextraction Gc–Fid Using Experimental Design. Journal of Analytical Chemistry, 72(3), 264-271.

Chicago

Masoumi V, Mohammadi A, Khoshayand MR, Ansari M. "Application of Polyaniline–Multiwalled Carbon Nanotubes Composite Fiber for Determination of Benzaldehyde in Injectable Pharmaceutical Formulations by Solid-Phase Microextraction Gc–Fid Using Experimental Design." Journal of Analytical Chemistry 72, no. 3 (2017): 264-271.

Harvard

Masoumi V et al. (2017) 'Application of Polyaniline–Multiwalled Carbon Nanotubes Composite Fiber for Determination of Benzaldehyde in Injectable Pharmaceutical Formulations by Solid-Phase Microextraction Gc–Fid Using Experimental Design', Journal of Analytical Chemistry, 72(3), pp. 264-271.

Vancouver

Masoumi V, Mohammadi A, Khoshayand MR, Ansari M. Application of Polyaniline–Multiwalled Carbon Nanotubes Composite Fiber for Determination of Benzaldehyde in Injectable Pharmaceutical Formulations by Solid-Phase Microextraction Gc–Fid Using Experimental Design. Journal of Analytical Chemistry. 2017;72(3):264-271.

BibTex

@article{ author = {Masoumi V and Mohammadi A and Khoshayand MR and Ansari M}, title = {Application of Polyaniline–Multiwalled Carbon Nanotubes Composite Fiber for Determination of Benzaldehyde in Injectable Pharmaceutical Formulations by Solid-Phase Microextraction Gc–Fid Using Experimental Design}, journal = {Journal of Analytical Chemistry}, volume = {72}, number = {3}, pages = {264-271}, year = {2017} }

RIS

TY - JOUR
AU - Masoumi V
AU - Mohammadi A
AU - Khoshayand MR
AU - Ansari M
TI - Application of Polyaniline–Multiwalled Carbon Nanotubes Composite Fiber for Determination of Benzaldehyde in Injectable Pharmaceutical Formulations by Solid-Phase Microextraction Gc–Fid Using Experimental Design
JO - Journal of Analytical Chemistry
VL - 72
IS - 3
SP - 264
EP - 271
PY - 2017
ER -

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