Optimization of a Methodology for Determination of Iron Concentration in Aqueous Samples Using a Newly Synthesized Chelating Agent in Dispersive Liquid-Liquid Microextraction

Optimization of a Methodology for Determination of Iron Concentration in Aqueous Samples Using a Newly Synthesized Chelating Agent in Dispersive Liquid-Liquid Microextraction Publisher

Borzoei M^{1, 2} ; Zanjanchi MA¹ ; Sadeghialiabadi H² ; Saghaie L²

Show Affiliations

1. Department of Chemistry, Faculty of Science, University of Guilan, Rasht, 41335-1914, Iran
2. Department of Medicinal Chemistry, Faculty of Pharmacy, Isfahan University of Medical Sciences, Isfahan, 81746-73461, Iran

Source: Food Chemistry Published:2018

Abstract

The aim of this study was to establish a new dispersive liquid-liquid microextraction (DLLME) technique for the determination of iron concentration in aqueous solutions and fruit juices based on the reaction between iron and 3-hydroxy-1-(3-hydroxyphenyl)-2-methylpyridin-4(1H)-one (3-OH-PMPO) as a chelating agent. A central composite design (CCD) was applied to optimize the effects of independent parameters (pH, volume of disperser solvent and extractant solvent and chelating agent concentration) on extraction efficiency. Under the optimized conditions, the analytical curve is linear in a concentration range of 10–750 μgL−1 with a detection limit of 5 μgL−1. The relative standard deviation (RSD) for ten repeated determinations of iron concentrations at 40 and 200 μgL−1 was calculated to be 4.2% and 1.2%, respectively. Relative recovery of iron in several water samples was investigated and the average was obtained in the range of 91–108%. © 2018 Elsevier Ltd

2. A New Spectrophotometric Method for Direct Determination of Iron (Iii) in Serum, Daru (2008)

3. Determination of Some B Vitamins in Sour Cherry Juice Using Dispersive Liquid-Liquid Microextraction Followed by High-Performance Liquid Chromatography, Iranian Journal of Pharmaceutical Research (2014)

4. Introduction and Review of Liquid-Liquid Microextraction Method, Development and Applications in Sample Preparation and Extraction, Journal of Health System Research (2022)

5. Introduction and Review of Techniques, Applications, and Limitations of Solid Phase Microextraction Method, Journal of Health System Research (2023)

6. Simultaneous Analysis of Benzoic and Sorbic Acids in Orange Juice Using Thymol/ Water Natural Deep Eutectic Solvent and Dllme Method Followed by High Performance Liquid Chromatography, Journal of Food Measurement and Characterization (2024)

7. Nife2o4 Nanoparticles Grafted Sulfonated Melamine for Rapid Magnetic Dispersive Μ-Solid Phase Extraction of Pesticides in Apple and Pear Samples: Greenness Evaluation, Microchemical Journal (2024)

8. Determination of Parabens in Wastewater and Sludge in a Municipal Wastewater Treatment Plant Using Microwave-Assisted Dispersive Liquid-Liquid Microextraction Coupled With Gas Chromatography-Mass Spectrometry, Environmental Health Engineering and Management (2019)

Experts (# of related papers)

View all Related Experts

Lotfollah Saghaie Dehkordi (2)

Sara Karimi Zeverdegani (2)

Style	Citing Format
MLA	Borzoei M, et al.. "Optimization of a Methodology for Determination of Iron Concentration in Aqueous Samples Using a Newly Synthesized Chelating Agent in Dispersive Liquid-Liquid Microextraction." Food Chemistry, vol. 264, no. , 2018, pp. 9-15.
APA	Borzoei M, Zanjanchi MA, Sadeghialiabadi H, Saghaie L (2018). Optimization of a Methodology for Determination of Iron Concentration in Aqueous Samples Using a Newly Synthesized Chelating Agent in Dispersive Liquid-Liquid Microextraction. Food Chemistry, 264(), 9-15.
Chicago	Borzoei M, Zanjanchi MA, Sadeghialiabadi H, Saghaie L. "Optimization of a Methodology for Determination of Iron Concentration in Aqueous Samples Using a Newly Synthesized Chelating Agent in Dispersive Liquid-Liquid Microextraction." Food Chemistry 264, no. (2018): 9-15.
Harvard	Borzoei M et al. (2018) 'Optimization of a Methodology for Determination of Iron Concentration in Aqueous Samples Using a Newly Synthesized Chelating Agent in Dispersive Liquid-Liquid Microextraction', Food Chemistry, 264(), pp. 9-15.
Vancouver	Borzoei M, Zanjanchi MA, Sadeghialiabadi H, Saghaie L. Optimization of a Methodology for Determination of Iron Concentration in Aqueous Samples Using a Newly Synthesized Chelating Agent in Dispersive Liquid-Liquid Microextraction. Food Chemistry. 2018;264():9-15.
BibTex	@article{ author = {Borzoei M and Zanjanchi MA and Sadeghialiabadi H and Saghaie L}, title = {Optimization of a Methodology for Determination of Iron Concentration in Aqueous Samples Using a Newly Synthesized Chelating Agent in Dispersive Liquid-Liquid Microextraction}, journal = {Food Chemistry}, volume = {264}, number = {}, pages = {9-15}, year = {2018} }
RIS	TY - JOUR AU - Borzoei M AU - Zanjanchi MA AU - Sadeghialiabadi H AU - Saghaie L TI - Optimization of a Methodology for Determination of Iron Concentration in Aqueous Samples Using a Newly Synthesized Chelating Agent in Dispersive Liquid-Liquid Microextraction JO - Food Chemistry VL - 264 IS - SP - 9 EP - 15 PY - 2018 ER -

Science Communicator Platform

Authors

Authors Affiliations

Abstract