Tehran University of Medical Sciences

Science Communicator Platform

Stay connected! Follow us on X network (Twitter):
Share this content! On (X network) By
Taguchi Approach-Assisted Optimization of Spraying in Non-Solvent Process for Preparation of Potassium Perchlorate Nanoparticles Publisher



Pourmortazavi SM1 ; Zaree A1 ; Mirsadeghi S2
Authors
Show Affiliations
Authors Affiliations
  1. 1. Malek Ashtar University of Technology, P. O. Box 16765-3454, Tehran, Iran
  2. 2. Nanotechnology Research Center, School of Pharmacy, Tehran University of Medical Science, Tehran, 1417614411, Iran

Source: Journal of Sol-Gel Science and Technology Published:2015


Abstract

In this study, Taguchi robust design as a statistical route was utilized to optimize the variables of spraying in non-solvent process in order to achieve KClO4 nanoparticles. The experimental factors of the spraying in non-solvent technique, which may be effective in KClO4 particle size, were optimized efficiently via Taguchi method. The procedure operating conditions, i.e., KClO4 concentration, solvent ratio, non-solvent identity, and spray steps, were considered at triple levels. The role of these operating conditions on the size of resulted KClO4 particles was evaluated quantitatively by analysis of variance (ANOVA). It was found that the particle size of KClO4 prepared by spraying in non-solvent technique might be adjusted efficiently by tuning the main parameters at the corresponding optimum level. Moreover, the optimal conditions for the preparing of KClO4 nanoparticles via the studied method were proposed. The ANOVA exhibited that 3 % (w/v) as KClO4 concentration, CHCl3 as type of non-solvent, solvent to non-solvent ratio of 1:6, and single-step spraying are optimal conditions for the production of KClO4 nanoparticles by spraying in non-solvent. Experimental data revealed that at optimum conditions of the process, the average particle size of produced KClO4 is about 41 nm. Meantime, KClO4 nanoparticles were prepared by supercritical carbon dioxide anti-solvent process for comparison. It was found that the size of the produced KClO4 particles is about 55 nm. Graphical Abstract: [Figure not available: see fulltext.] © 2015, Springer Science+Business Media New York.
Related Docs
View other Related Docs
1. Electrochemical Synthesis of Copper Carbonates Nanoparticles Through Experimental Design and the Subsequent Thermal Decomposition to Copper Oxide, Materials Research Express (2019)
2. Rapid Photodegradation and Detection of Zolpidem Over Β-Snwo4 and Α-Snwo4 Nanoparticles: Optimization and Mechanism, Environmental Science and Pollution Research (2021)
3. Green and Simple Synthesis of Silver Nanoparticles by Aqueous Extract of Perovskia Abrotanoides: Characterization, Optimization and Antimicrobial Activity, Current Pharmaceutical Biotechnology (2020)
4. Synthesis of Sm2(Wo4)3 Nanocrystals Via a Statistically Optimized Route and Their Photocatalytic Behavior, Materials Research Express (2017)
5. In Vitro Antibacterial Property Assessment of Silver Nanoparticles Synthesized by Falcaria Vulgaris Aqueous Extract Against Mdr Bacteria, Journal of Sol-Gel Science and Technology (2019)
6. Optimizing the Synthesis of Terbium(Iii) Molybdate Nanoplates Through an Orthogonal Array Design, Environmental Progress and Sustainable Energy (2019)
7. Photocatalytic Reduction of Imatinib Mesylate and Imipenem on Electrochemical Synthesized Al2w3o12 Nanoparticle: Optimization, Investigation of Electrocatalytic and Antimicrobial Activity, Colloids and Surfaces A: Physicochemical and Engineering Aspects (2020)
8. Optimized Routes for the Preparation of Gadolinium Carbonate and Oxide Nano-Particles and Exploring Their Photocatalytic Activity, Desalination and Water Treatment (2017)
Experts (# of related papers)
Bagher Larijani (1)
Other Related Docs
9. Synthesis, Characterization and Photocatalytic Activity of Neodymium Carbonate and Neodymium Oxide Nanoparticles, Journal of Molecular Structure (2017)
10. Optimizing the Procedure for the Synthesis of Nanoscale Gadolinium(Iii) Tungstate As Efficient Photocatalyst, Journal of Materials Science: Materials in Electronics (2017)
11. Supercritical Fluid Extraction of Pesticides and Insecticides From Food Samples and Plant Materials, Critical Reviews in Analytical Chemistry (2021)
12. Erbium(Iii) Tungstate Nanoparticles; Optimized Synthesis and Photocatalytic Evaluation, Journal of Materials Science: Materials in Electronics (2017)
13. Facile and Effective Synthesis of Praseodymium Tungstate Nanoparticles Through an Optimized Procedure and Investigation of Photocatalytic Activity, Open Chemistry (2017)
14. Synthesis, Characterization, and Photocatalytic Behavior of Praseodymium Carbonate and Oxide Nanoparticles Obtained by Optimized Precipitation and Thermal Decomposition, Journal of Electronic Materials (2017)
15. Samarium Carbonate and Samarium Oxide; Synthesis, Characterization and Evaluation of the Photo-Catalytic Behavior, Journal of Materials Science: Materials in Electronics (2017)
16. Fabrication of Fe3o4 Nanoparticles Coated by Extracted Shrimp Peels Chitosan As Sustainable Adsorbents for Removal of Chromium Contaminates From Wastewater: The Design of Experiment, Composites Part B: Engineering (2019)
17. Preparation of Dysprosium Carbonate and Dysprosium Oxide Efficient Photocatalyst Nanoparticles Through Direct Carbonation and Precursor Thermal Decomposition, Journal of Materials Science: Materials in Electronics (2017)
18. Application of Taguchi Robust Design to the Optimization of the Synthesis of Holmium Carbonate and Oxide Nanoparticles and Exploring Their Photocatalyst Behaviors for Water Treatment, Journal of Materials Science: Materials in Electronics (2017)